Nuclear Magnetic Resonance Studies of Interfacial Phenomena

By (author) Gun'ko, Vladimir M.; By (author) Turov, Vladimir V.

Properties and applications of high surface area materials depend on interfacial phenomena, including diffusion, sorption, dissolution, solvation, surface reactions, catalysis, and phase transitions. Among the physicochemical methods that give useful information regarding these complex phenomena, nuclear magnetic resonance (NMR) spectroscopy is the most universal, yielding detailed structural data regarding molecules, solids, and interfaces. Nuclear Magnetic Resonance Studies of Interfacial Phenomena summarizes NMR research results collected over the past three decades for a wide range of materials-from nanomaterials and nanocomposites to biomaterials, cells, tissues, and seeds. This book describes the applications of important new NMR spectroscopic methods to a variety of useful materials and compares them with results from other techniques such as adsorption, differential scanning calorimetry, thermally stimulated depolarization current, dielectric relaxation spectroscopy, infrared spectroscopy, optical microscopy, and small-angle and wide-angle x-ray scattering. The text explores the application of NMR spectroscopy to examine interfacial phenomena in objects of increasing complexity, beginning with unmodified and modified silica materials. It then describes properties of various mixed oxides with comparisons to individual oxides and also describes carbon materials such as graphite and carbon nanotubes. Chapters deal with carbon-mineral hybrids and their mosaic surface structures, and interfacial phenomena at the surface of natural and synthetics polymers. They also explore a variety of biosystems, which are much more complex, including biomacromolecules (proteins, DNA, and lipids), cells and tissues, and seeds and herbs. The authors cover trends in interfacial phenomena investigations, and the final chapter describes NMR and other methods used in the book. This text presents a comprehensive description of a large array of hard and soft materials, allowing the analysis of the structure-property relationships and generalities on the interfacial behavior of materials and adsorbates.

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  • Unmodified and Modified Silicas Interfacial Phenomena at a Surface of Nanosilica Silica gels, Aerogels, Silochrome, and Poly(methylsiloxane): Structural, Interfacial and Adsorption Characteristics, and Structure-Property Relationships Interfacial Phenomena at Surfaces of Structurally Ordered Silicas Thin Films and Other Moieties on Silica Supports Interfacial Phenomena at Surfaces of Mixed Oxides Mixed Nanooxides Porous Oxides as a Function of Morphology Structurally Ordered Oxides Nanocrystalline and Microcrystalline Materials Clays, Zeolites, and Other Natural Minerals Interfacial Phenomena at Surfaces of Carbon Materials Texture of Carbonaceous Materials and Chemical Shift of Adsorbed Molecules Activated Carbons Graphitized Carbons and Graphite Carbon Nanotubes Interfacial Phenomena at Carbon-Mineral Composites Carbon Blacks Carbonized Silicas and Mixed Oxides Interfacial Phenomena at Polymer Surfaces Natural Polymers: Cellulose, Starch, Chitosan, Hyaluronic Acid, and Others Synthetic Polymers Hydrogels and Cryogels Polymer-Nanooxide Systems Polymers in Confined Space of Pores Interactions of Biomacromolecules with Water, Organic Compounds, and Oxides, Polymers, and Carbon Adsorbents Proteins Proteins in Adsorbed State DNA Lipids Water Associated with Bio-Objects: Cells and Tissues Yeast Saccharomyces cerevisiae Cells Intracellular Water in Partially Dehydrated Bone Marrow Cells Freeze-Dried Bovine Gametes with Organic Additives Red Blood Cells Bone Tissue Muscular Tissues Intracellular Water and Cryopreservation Interaction of Seeds, Herbs, and Related Materials with Water and Nanooxides Recurring Trends in Adsorption, Spectroscopy, and Other Interfacial Experiments Methods Low-Temperature 1H NMR Spectroscopy Low-Temperature Nitrogen Adsorption Adsorption of Water and Organics Polymer and Protein Adsorption Infrared Spectroscopy Thermogravimetry Differential Scanning Calorimetry Auger Electron Spectroscopy Temperature-Programmed Desorption with Mass-Spectrometry Control Thermally Stimulated Depolarization Current Dielectric Relaxation Spectroscopy Ultraviolet-Visible Spectroscopy Rheometry Potentiometric Titration Photon Correlation Spectroscopy Adsorption of Metal Ions X-Ray Diffraction Raman Spectroscopy AFM, SEM, and TEM Quantum Chemistry Conclusions

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書名 Nuclear Magnetic Resonance Studies of Interfacial Phenomena
著作者等 Turov, Vladimir V.
Gun'ko, Vladimir M.
シリーズ名 Surfactant Science Series
出版元 Taylor & Francis Inc
刊行年月 2013.04.23
ページ数 1040p
ISBN 9781466551695
言語 英語
出版国 アメリカ合衆国